《Spectrometric Identification of Organic Compounds》第七版
波谱分析最经典的一本书,网上很多地方都有电子版提供(扫描的,效果挺好,挺清晰),发出来与大家分享。Spectrometric Identification of Organic Compounds, 7th Edition
Robert M. Silverstein, Francis X. Webster, David Kiemle
ISBN: 978-0-471-39362-7
Hardcover
512 pages
January 2005
Wiley List Price: US $134.95
This price is valid for China.
简介:
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book:
* Uses a problem-solving approach with extensive reference charts and tables.
* Offers an extensive set of real-data problems offers a challenge to the practicing chemist
目录:
Chapter 1. Mass Spectrometry.
1.1 Introduction.
1.2 Instrumentation.
1.3 Ionization Methods.
1.4 Mass Analyzers.
1.5 Interpretation of El Mass Spectra.
1.6 Mass Spectra of Some Chemical Classes.
Chapter 2. Infrared Spectrometry.
2.1 Introduction.
2.2 Theory.
2.3 Instrumentation.
2.4 Sample Handling.
2.5 Interpretations of Spectra.
2.6 Characteristic Group Absorption of Organic Molecules.
Chapter 3. Proton Magnetic Resonance Spectrometry.
3.1 Introduction.
3.2 Theory.
3.3 Instrumentation and Sample Handling.
3.4 Chemical Shift.
3.5 Spin Coupling, Multiplets, Spin Systems.
3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons.
3.7 Coupling of Protons to Other Important Nuclei (<sup>19</sup>F, E, <sup>31</sup>P, <sup>29</sup>Si, and <sup>13</sup>C.
3.8 Chemical Shift Equivalence.
3.9 Magnetic Equivalence (Spin-Coupling Equivalence).
3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants.
3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling.
3.12 Chirality.
3.13 Vicinal and Geminal Coupling.
3.14 Low-Range Coupling.
3.15 Selective Spin Decoupling. Double Resonance.
3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space.
Chapter 4. Carbon-13 NMR Spectrometry.
4.1 Introduction.
4.2 Theory.
4.3 Interpretation of a Simple <sup>13</sup>C Spectrum: Diethyl Phthalate.
4.4 Quantitative <sup>13</sup>C Analysis.
4.5 Chemical Shift Equivalence.
4.6 DEPT.
4.7 Chemical Classes and Chemical Shifts.
Chapter 5. Correlation NMR Spectrometry; 2-D NMR.
5.1 Introduction.
5.2 Theory.
5.3 Correlation Spectrometry.
5.4 Ipsenol: <sup>1</sup>H-<sup>1</sup>H COSY.
5.5 Caryophyllene Oxide.
5.6 <sup>13</sup>C-<sup>13</sup>C Correlations: Inadequate.
5.7 Lactose.
5.8 Relayed Coherence Transfer: TOCSY.
5.9 HMQC – TOCSY.
5.10 ROESY.
5.11 VGSE.
5.12 Gradient Field NMR.
Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei.
6.1 Introduction.
6.2 <sup>15</sup>N Nuclear Magnetic Resonance.
6.3 <sup>19</sup>F Nuclear Magnetic Resonance.
6.4 <sup>29</sup>Si Nuclear Magnetic Resonance.
6.5 <sup>31</sup>P Nuclear Magnetic Resonance.
6.6 Conclusion.
Chapter 7. Solved Problems.
7.1 Introduction.
Chapter 8. Assigned Problems.
8.1 Introduction.
[url]http://rapidshare.com/files/14294544/spectrometric_identification_of_organic_compunds_7th_ed_silverstein_2005.pdf[/url] :victory: :handshake 谢谢楼主介绍,但是下载不了 亲爱的楼主,能在给传下么,现在下载不了啊 下不了啊
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